A 100% Water Mobile Phase HPLC-PDA Analysis of Selected Neonicotinoid Insecticides

Authors

  • Naoto Furusawa Graduate School of Human Life Science, Osaka City University

DOI:

https://doi.org/10.24297/jac.v10i9.878

Keywords:

Internal harmonized analytical method, Acetamiprid, Imidacloprid, High-Performance Liquid Chromatography, Photo-diode array

Abstract

This paper describes a reserved-phase HPLC method for detecting frequently-used neonicotinoid insecticides, acetamiprid (ATP) and imidacloprid (ICP), using an isocratic 100 % water mobile phase.  Chromatographic separations were performed an Inertsil® WP300 C4 with water mobile phase and a photodiode-array detector.  The total run time was < 7 min.  The system suitability was well within the international acceptance criteria.  The detection limits were 0.013 μg ml-1 for ATP and 0.015 μg ml-1 for ICP, respectively.  A harmless HPLC method for simultaneous detecting ATP and ICP was developed and may be further applied to the quantification in foods.

 

 

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Published

2014-11-26

How to Cite

Furusawa, N. (2014). A 100% Water Mobile Phase HPLC-PDA Analysis of Selected Neonicotinoid Insecticides. JOURNAL OF ADVANCES IN CHEMISTRY, 10(9), 3127-3132. https://doi.org/10.24297/jac.v10i9.878

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Articles