Synthesis and characterization of a new Organic – Inorganic sulfate (C5H6N2O)2[Co(H2O)6]3(SO4)4.2H2O
DOI:
https://doi.org/10.24297/jac.v10i4.5505Keywords:
Organic-inorganic hybrid, Crystal structure, IR Spectroscopy, Band-gap.Abstract
crystals of a new hybrid compound, (C5H6N2O)2[Co(H2O)6]3(SO4)4.2H2O, were synthesized in aqueous solution and characterized. This compound crystallizes in the triclinic system with the space group P-1, the unit cell :a=6.632(3) Ã…, b=11.769(5) Ã…, c=14.210(6) Ã…, α=67.86(4)°, β=81.32(4)°, γ=85.18(4)° and V=1015.14(8) Ã…3 . Its crystal structure can be described as a packing of alternated inorganic and organic layers. The different components are connected by a three-dimensional network of O-H…O and N-H…O hydrogen bonds.Â
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