Effect of MWCNT doping on the structural and optical properties of PVC/PVDF polymer blend
DOI:
https://doi.org/10.24297/jap.v13i2.5702Keywords:
MWCNTs, PVDF/PVC blend, TEM, FTIRAbstract
Thin film samples of pristine polyvinyl chloride (PVC), poly vinyldine fluoride (PVDF) in combination with their blend in addition to samples containing factorial mass fraction of multi wall carbon nano-tubes (MWCNTs) in the dopant level were prepared via routine casting technique using tetrahydrofurane (THF) as a common solvent. X-ray diffraction and transmission electron microscopy (TEM) depict the nano-scale (15-25 nm) of functionalized MWCNTs with no surface damage results from functionalization process.X-ray diffraction (XRD) shows a semi-crystalline nature of PVDF with evidence for more than one phase namely a and b phases. The fraction of b phase was calculated and correlated to the dopant content. FTIR optical absorption spectra revels a preservation of the main vibrational bands before and after addition of MWCNTs in the doping level with a presence of new small band 1151 cm-1 assigned for the interaction and complexation between constituents.Downloads
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References
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3. T. Khadiran, M.Z. Hussein, Z. Zainal, R. Rusli (2016), Renewable and Sustainable Energy Reviews 57, 916-928.
4. J. Stampfl, R. Liska (2005) Macromol. Chem. Phys. 206, 1253–1256.
5. V. Popa, S. Dumitriuv, (2013) Polymeric Biomaterials: Structure and Function, Taylor and Francis Group, CRC Press.
6. S.K. Misra, F. Ohashi, S.P. Valappil, J.C. Knowles, I. Roy, S.R. Silva, V. Salih, A.R. Boccaccini (2010) Acta Biomater. 6(3), 735-742.
7. X.H. Xia, Z.I Jia, Y. Yu, Y. Liang, Z. Wang, L.L. Ma (2007), Carbon 45(4), 717-721.
8. A.M. Abdelghany, E.M. Abdelrazek, A.H. Oraby, E. Lasheen (2013) Research Journal of Pharmaceutical, Biological and Chemical Sciences 4,565-76.
9. J.M. Brynaet, N. Jongen, J.L. Dewez (1997) J. Polym. Sci. Polym. Chem. 35, 1227-1235.
10. D.W. van Krevelen, K.T. Nijenhuis (2009) Properties of polymers: their correlation with chemical structure; their numerical estimation and prediction from additive group contributions. 4th edition, Elsevier.
11. D.Q. Yang, J.F. Rochette, E. Sacher, (2005). J. Phys. Chem. B, 109, 7788-7794.
12. A. Hartono, S. Satira, M. Djamal, R. Ramli, H. Bahar, E. Sanjaya, (2013) Advances in Materials Physics and Chemistry 3, 71-76.
13. A. Allaoui, S. Bai, H.M. Cheng, J.B. Bai (2002) Composites Science and Technology 62, 1993–1998.
14. JrR. Gregorio (2006) J. Appl. Polym. Sci. 100(4), 3272-3279.
15. J. Wu, T. Chen, X. Luo, D. Han, Z. Wang, J. Wu (2014), Waste Management 34(3), 676-682.
16. S. Ramesh, Koay Hang Leen, K. Kumutha, A.K. Arof (2007) Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 66(4-5)1237-1242.
17. A. M. Abdelghany, E. M. Abdelrazek, A. ElShahawy and A. A. Al-Muntaser (2015) Middle East Journal of Applied Sciences, 5(5), 36-44.
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Published
2017-02-16
How to Cite
Abdelghany, A. M., Meikhail, M., Badr, S., & Momen, A. S. (2017). Effect of MWCNT doping on the structural and optical properties of PVC/PVDF polymer blend. JOURNAL OF ADVANCES IN PHYSICS, 13(2), 4640–4647. https://doi.org/10.24297/jap.v13i2.5702
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