A Novel Synthesis of (Z)-ethyl 3-amino-2-cyano-3-phenyl(or alkyl)acrylate and ethyl- 2-cyano-3-phenyl-3-propionylimino-propanoate
Keywords:Imidate, N-acetyl imidate, N-ethoxycarbonyl imidate, ethyl cyanoacetate, X-ray diffraction, H-bonds.
Reaction between ethyl cyanoacetate and imidate, N-acetyl imidate and N-ethoxycarbonyl imidate in basic medium are student. The structure and geometrically configuration of (Z)-ethyl 3-amino-2-cyano-4-phenylbut-2-enoate 3c was established by X-ray diffraction. The functionality in ethyl 2-cyano-3-(ethoxycarbonyl)-3-p-tolylacrylate 7b was exploited to get the desired heterocycle.Â Â
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