Synthesis and vibrational study of phosphate-sulfate fluorapatites Ca10-xNax(PO4)6-x(SO4)xF2 (0≤ x ≤6)
DOI:
https://doi.org/10.24297/jac.v12i17.1418Keywords:
Sulfate fluorapatite, X-ray diffraction, Infrared absorption, Raman scattering spectroscopy.Abstract
   A series of phosphate-sulfate fluorapatites Ca10-xNax(SO4)x(PO4)6-xF2 has been synthesized by the solid-state reaction at high temperature. The samples were characterized using X-ray diffraction, Infrared spectroscopy and Raman scattering spectroscopy. X-ray diffraction study shows that these materials crystallize in the hexagonal system with P63/m as space group. Infrared and Raman spectra are reported and band assignments are made.Â
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[7] Tonsuaadu K., Peld M., Quarton M., Bender V., Veiderma M., J. Oganometall. Chem. 177 (2002) 1873.
[8] Laghzizil A., El Hajjaji S., Bouhaouss A., Ferhat M. Solid State Ionics. 126 (1999) 245.
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[21] Frost R. L., Wills R. A., Weier M. L., Martens W., Kloprogge J. T. J. Mol. Struct. 785 (2006) 123.
[22] Rudolph W.W., Mason R.J. Solution Chem. 30 (2001) 527.
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Published
2016-09-01
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Synthesis and vibrational study of phosphate-sulfate fluorapatites Ca10-xNax(PO4)6-x(SO4)xF2 (0≤ x ≤6). (2016). JOURNAL OF ADVANCES IN CHEMISTRY, 12(17), 4975–4980. https://doi.org/10.24297/jac.v12i17.1418
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